陈耀祖院士研究论文选PDF格式文档图书下载

第1篇 质谱分析的研究与应用 3

1-1 Reaction Mass Spectrometry 3

1-2 Stereochemical Effects in Mass Spectrometry 2-Chemical Ionization Mass Spectra of Some Cyclic Glycols and Mono-and Di-saccharides Using Trimethyl Borate as Reagent Gas 19

1-3 Stereochemical Effects in Mass Spectrometry 3 Detection of Chirality by Che-mical Ionization Mass Spectrometry 27

1-4 Stereochemical Studies on Steroids by Mass Spectrometry(Ⅳ)：-Application of Me3SiNEt2 as a Reagent 33

1-5 Stereochemical Effects in Mass Spectra-Studies on Mass Spectra of Epimers of Podophyllotoxin and Its Derivatives 36

1-6 Stereochemical Effects in Mass Spectrometry 43

1-7 Mass Spectrometry of Natural Products Stereochemical Studies by Reaction Mass Spectrometry 49

1-8 CI Mass Spectra of Substituted Phenols with Acetone as Reagent 52

1-9 Stereochemical Effects in Mass Spectrometry：Part 8—Chemical Ionization Mass Spectra of Cyclic Glycols and Monosaccharides Using Formaldehyde Dimethyl Acetal as Reagent Gas 54

1-10 Stereochemical Effects in Mass Spectrometry Part 10 Reaction Mass Spectrometry of Cyclic Glycols and Monosaccharides with Methylene Chloride as Reagent Gas 61

1-11 反应质谱法——超微量立体化学分析新技术 67

1-12 天然有机化合物 77

1-13 Stereochemical Effects in Mass Spectrometry ⅩⅢ Determination of Absolute Configuration by Fast Atom Bombardment Mass Spectrometry 82

1-14 Stereochemical Effects in Mass Spectrometry ⅩⅤ Chemical Ionization of Some Substituted Alkenes Using Dichlorocarbene as the Reagent Gas 90

1-15 Association of the Acylium Ion of Acids with Alcohols as an Esterification Mechanism in Chemical Ionization 95

1-16 Stereochemical Effects in Mass Spectrometry-Determination of the Optical Purity of Enantiomers by Mass Spectrometry 97

1-17 快原子轰击和碰撞活化质谱法研究三萜皂苷结构 102

1-18 Fast Atom Bombardment and Collisional Activation Mass Spectrometry in the Structural Analysis of Steroidal Oligoglycosides 106

1-19 Studies on the mass spectrometry of natural products 115

1-20 天然有机化合物质谱研究 121

1-21 寡糖快原子轰击质谱中碱金属加合离子应用技术的研究 130

1-22 Mass Spectrometry of Oligosaccharides(Ⅰ)-Formation of theM+NH4］+ Ion of Oligosaccharides in Fast Atom Bombardment Mass spectrometry 133

第2篇 天然产物化学 139

2-1 当归化学成分分析研究——毛细管气相色谱-质谱法鉴定当归根挥发油成分 139

2-2 Analysis of Chemical Ingredients of Angelica Sinensis——Analysis of Non-Volatile Constituents of Roots 144

2-3 细花雪胆中的新成分——新葫芦素 152

2-4 Determination of Volatile Constituents of Chinese Medicinal Herbs by Direct Vaporization Capillary Gas Chromatography/Mass Spectrometry 156

2-5 Diterpenoid Alkaloids of Aconitum Sungpanense 167

2-6 Diterpenoids From Rabdosia Henryi 173

2-7 Ganschisandrine，A Lignan from Schisandra Sphenanthera 178

2-8 Diterpenoids from RabdosiaJaponica Var.Glaucocalyx 181

2-9 Diterpenoid Alkaloids from Delphinium Winklerianum 185

2-10 A Diterpenoid Alkaloid from Aconitum Vilmorinianum Var.Patentipilum 191

2-11 Bioactive Sesquiterpene Polyol Esters from Euonymus Bungeanus 195

2-12 Diterpenoids from Rabdosia Pseudo-Irrorata 202

2-13 Diterpenoid Alkaloids from Aconitum Vilmorrianum 208

2-14 Sesquiterpene Polyol Esters from Celastrus Paniculatus 213

2-15 Dihydroagarofuran Sesquiterpenoids from Celastrus Panicula Tus 218

2-16 Diterpenoids from Rabdosia ParVifolia 224

2-17 Diterpenoid Alkaloids from Delphinium caeruleum 229

2-18 Triterpenoid Saponins from Anemone Hupehensis 234

2-19 Diterpenoid Alkaloids from Aconitum Talassicum 240

2-20 Oligostilbenes from Vitis Heyneana 247

2-21 Diterpenoid Alkaloids from Delphinium Caeruleum 252

2-22 Triterpenoid Saponins from Anemone Hupehensis 256

2-23 Diterpenoids from Isodon Gesneroides 261

2-24 TwoNewSesquiterpenes from CelastrusAngulatus 268

2-25 Souline C and Souline D，New Diterpenoid Alkaloids From Delphinium Souliei 272

2-26 A Simplified and Practical Method for Methylation Analysis of Polysaccharides 275

2-27 红芪多糖RHG的分离纯化及化学结构 278

2-28 Diterpenoids from Isodon Leucophyllus 282

2-29 Diterpenoids from Isodon Eriocalyx 288

2-30 Phenylpropanoid Glycosides from LamiophlomisRotata 294

2-31 滇姜花抗肿瘤活性二萜及其光敏氧化反应的研究 299

2-32 ent-Kaurene diterpenoids from Isodon Rubescens 303

2-33 Two Glycosides from the Stem Bark of Tetracentron sinense 309

2-34 Two New Diterpenoids from Isodon Rubescens 314

2-35 卵叶银莲花全草中的新三萜皂苷 316

第3篇 有机分析 325

3-1 Microidentification of Aldehydes andAnines 325

3-2 Two New Solvents for the Rast Method of Microdetermination of Molecular Weights 332

3-3 原子吸收光度法测定还原糖和脂肪仲胺 334

3-4 Study on Spin Labeling Analysis Synthesis and ESR Determination of Spin-Labeled Anti-Tumour Podophyllotoxin Derivatives 337

3-5 Two-dimensional NMR Study of Ganwuweizic Acid 340

3-6 Separation of Polycyclic Aromatic Hydrocarbons by Micellar E1ectrokinetic Chromatography with Aqueous Short-Chain Alcohol Solvent 346

3-7 Chiral Gas Chromatographic Assay with Flame Ionization Detection for Amphetamine Enantiomers in Microsomal Incubates 353

3-8 Carboxymethyl-β-Cyclodextrin for Chiral Separation of Basic Drugs by Capillary Electrophoresis 359

第4篇 有机化学 369

4-1 苯甲酰异硫氰用作鉴定醇类的试剂 369

4-2 磺胺苯并噻唑Ⅳ.具有羧基的磺胺苯并噻唑 371

4-3 甲基硅烷的气相氯化 377

4-4 Acylthiosemicarbazides and Related Compounds 382

4-5 The Total Synthesis of Taxamairin B 386

4-6 The First Total Synthesis of(±)-Demethyl Salvicanol 392

4-7 A Facial One-step Approach to Stereospecific Spirocyclic Diols from α-Hydroxy-epoxides 400

4-8 新的烯丙型环氧醇重排还原反应研究 403

4-9 An Efficient Synthesis of N-Trifluoroacetyl Adriamycin-14-Valerate(AD-32) 407

4-10 Synthesis of Heterocyclic Compounds from 2-Phenyl-1，2，3-Triazole-4-Formy-lhydrazine 410

第5篇 药物化学 419

5-1 Spin-Labeled Antitumor Derivatives of Podophy llotoxin 419

5-2 Anticancer Drugs Ⅱ.Synthesis and Biological Evaluation of Spin Labeled Deriv-atives of Podophyllotoxin 429

5-3 Anticancer Drugs Part Ⅲ：New Spin Labelled Derivatives of Podophyllotoxin 435

5-4 Synthesis and Antitumor Activity of Spin-Labeled Derivatives of Podophyllotoxin 439

5-5 Studies on Spin-Labelled Peptide Nucleic Acid 445

5-6 杂环化合物取代的5-氟尿嘧啶衍生物的合成及抗肿瘤活性 450

5-7 A Facile and Efficient Synthesis of 4β-Aminopodophyllotoxins 453

5-8 Synthesis of Novel 4β-(1，2，3-Triazol-1-y1)Podophyllotoxins as Potential Anti-tumor Drugs 457

5-9 Synthesis of Spin Labeled Carbocyclic Lignan Analogue Related to Podophyllo-toxin 461

5-10 The Synthesis of 6-Alkyl-5-Fluorouracil Derivatives 465

5-11 A Facile and Highly Stereoselective Reductive Debromination of Anhydro-6-(R)-Hydroxyethyl-6-Bromopenicillin 468

5-12 Synthesis of Novel Spin Labeled Analogues of N-(Trifluoroacetyl)-Daunorubicin 470

5-13 Synthesis of 1-Arylated Derivatives of 5-Fluorouracil As Potential Antitumor Drug 474

5-14 4β-氨基-4-脱氧鬼臼毒素和4β-氨基-4-脱氧-4′-去甲基鬼臼毒素的两种新合成方法 477

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